Synthesis and structures of [2n](2,7)naphthalenophanes (n = 2-4)

Kenta Ohtsuka, Guangke Cai, Kazuya Fujita, Hirokazu Miyoshi, Yoshito Tobe*

*Corresponding author for this work

研究成果: Article同行評審

1 引文 斯高帕斯(Scopus)

摘要

Reductive coupling of 2,7-bis(bromomethyl)naphthalene using phenyllithium gave anti-[22](2,7)naphthalenophane, [23](2,7)naphthalenophane, and [24](2,7)naphthalenophane, the distribution of which was dependent on the reaction conditions. The structure of the first compound was established by X-ray crystallographic analysis. On the basis of the similarity between the NMR and UV spectra of [23](2,7)naphthalenophane with those reported for syn-[22](2,7)naphthalenophane, we conclude that the compound originally assigned to be syn-4 was in fact 6.

原文English
頁(從 - 到)445-449
頁數5
期刊Canadian Journal of Chemistry
95
發行號4
DOIs
出版狀態Published - 1 一月 2017

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