Quick execution of [2+2] type photochemical cycloaddition reaction by continuous flow system using a glass-made microreactor

Takahide Fukuyama*, Yoshiko Hino, Naoya Kamata, Ilhyong Ryu

*Corresponding author for this work

研究成果: Article同行評審

95 引文 斯高帕斯(Scopus)

摘要

A photochemical [2+2] cycloaddition reaction was executed in a microflow system using glass-made microchannels having 1000-μm width and 500-μm depth. The reaction of cyclohexenones with vinyl acetates in a microflow system under irradiation (300 W, Hg lamp) gave [2+2] cycloaddition products in good yield with a residence time of 2 h, which is a remarkably shortened reaction time compared with a batch system using the same light source.

原文English
頁(從 - 到)1430-1431
頁數2
期刊Chemistry Letters
33
發行號11
DOIs
出版狀態Published - 5 十一月 2004

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