Quick execution of [2+2] type photochemical cycloaddition reaction by continuous flow system using a glass-made microreactor

Takahide Fukuyama; Yoshiko Hino; Naoya Kamata; Ilhyong Ryu

doi:10.1246/cl.2004.1430

Quick execution of [2+2] type photochemical cycloaddition reaction by continuous flow system using a glass-made microreactor

Takahide Fukuyama^*, Yoshiko Hino, Naoya Kamata, Ilhyong Ryu

^*Corresponding author for this work

Department of Applied Chemistry

Research output: Contribution to journal › Article › peer-review

95 Scopus citations

Abstract

A photochemical [2+2] cycloaddition reaction was executed in a microflow system using glass-made microchannels having 1000-μm width and 500-μm depth. The reaction of cyclohexenones with vinyl acetates in a microflow system under irradiation (300 W, Hg lamp) gave [2+2] cycloaddition products in good yield with a residence time of 2 h, which is a remarkably shortened reaction time compared with a batch system using the same light source.

Original language	English
Pages (from-to)	1430-1431
Number of pages	2
Journal	Chemistry Letters
Volume	33
Issue number	11
DOIs	https://doi.org/10.1246/cl.2004.1430
State	Published - 5 Nov 2004

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abstract = "A photochemical [2+2] cycloaddition reaction was executed in a microflow system using glass-made microchannels having 1000-μm width and 500-μm depth. The reaction of cyclohexenones with vinyl acetates in a microflow system under irradiation (300 W, Hg lamp) gave [2+2] cycloaddition products in good yield with a residence time of 2 h, which is a remarkably shortened reaction time compared with a batch system using the same light source.",

author = "Takahide Fukuyama and Yoshiko Hino and Naoya Kamata and Ilhyong Ryu",

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AU - Kamata, Naoya

AU - Ryu, Ilhyong

PY - 2004/11/5

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AB - A photochemical [2+2] cycloaddition reaction was executed in a microflow system using glass-made microchannels having 1000-μm width and 500-μm depth. The reaction of cyclohexenones with vinyl acetates in a microflow system under irradiation (300 W, Hg lamp) gave [2+2] cycloaddition products in good yield with a residence time of 2 h, which is a remarkably shortened reaction time compared with a batch system using the same light source.

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JO - Chemistry Letters

JF - Chemistry Letters

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ER -

Quick execution of [2+2] type photochemical cycloaddition reaction by continuous flow system using a glass-made microreactor

Abstract

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