Mizoroki-Heck arylation of α,β-unsaturated acids with a hybrid fluorous ether, F-626: Facile filtrative separation of products and efficient recycling of a reaction medium containing a catalyst

Takahide Fukuyama, Masashi Arai, Hiroshi Matsubara, Ilhyong Ryu*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

66 Scopus citations

Abstract

The Mizoroki-Heck reaction was carried out using a fluorous ether F-626 as the solvent and a fluorous Pd carbene complex as the catalyst. When carboxylic acids are the products, separation of both the F-626 and the Pd catalyst from the products can be conveniently carried out by simple filtration. The F-626 filtrates containing the Pd catalyst can be recycled.

Original languageEnglish
Pages (from-to)8105-8107
Number of pages3
JournalJournal of Organic Chemistry
Volume69
Issue number23
DOIs
StatePublished - 12 Nov 2004

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